ChemicalBook CAS DataBase List 1-[3-(2-hydroxypropan-2-yl)phenyl]ethanone

1-[3-(2-hydroxypropan-2-yl)phenyl]ethanone synthesis

3synthesis methods

Product Name:1-[3-(2-hydroxypropan-2-yl)phenyl]ethanone
CAS Number:87771-41-3
Molecular formula:C11H14O2
Molecular Weight:178.23

3-ISOPROPENYL-ALPHA,ALPHA-DIMETHYLBENZYL ISOCYANATE

2094-99-7
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1-[3-(2-hydroxypropan-2-yl)phenyl]ethanone

87771-41-3
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: ozone; oxygen / dichloromethane / -78 °C
1.2: 10 h / 20 °C
2.1: water; hydrogenchloride / Reflux; Inert atmosphere
3.1: chlorosulfonic acid / chloroform / 0.42 h / 0 °C / Inert atmosphere
4.1: potassium nitrite / Inert atmosphere
4.2: 3407 / 2 h / pH 2.8 / Inert atmosphere

References:

Gorla, Suresh Kumar;Kavitha, Mandapati;Zhang, Minjia;Liu, Xiaoping;Sharling, Lisa;Gollapalli, Deviprasad R.;Striepen, Boris;Hedstrom, Lizbeth;Cuny, Gregory D. [Journal of Medicinal Chemistry,2012,vol. 55,# 17,p. 7759 - 7771]

Ethanone, 1-[3-(1-isocyanato-1-methylethyl)phenyl]-

1397293-17-2
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87771-41-3
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References

Ethanone, 1-[3-(1-amino-1-methylethyl)phenyl]-

1397293-24-1
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87771-41-3
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References