ChemicalBook CAS DataBase List 1,3-BIS(4-HYDROXYBUTYL)TETRAMETHYLDISILOXANE

1,3-BIS(4-HYDROXYBUTYL)TETRAMETHYLDISILOXANE synthesis

9synthesis methods

Product Name:1,3-BIS(4-HYDROXYBUTYL)TETRAMETHYLDISILOXANE
CAS Number:5931-17-9
Molecular formula:C12H30O3Si2
Molecular Weight:278.54

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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1,3-BIS(4-HYDROXYBUTYL)TETRAMETHYLDISILOXANE

5931-17-9
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$60.00/100mg

Yield: 83.7%

Reaction Conditions:

with acetic acid in water;toluene; pH=2

Steps:

3.2; 3.3 Example 3,Preparation of 1,3-bis (hydroxybutyl) -1,1,3,3-tetramethyldisiloxane,The structural formula is as shown in formula (VI):
(2) A single-necked flask equipped with a constant pressure dropping funnel was charged with the product obtained in the step (1), to which a CH3COOH aqueous solution of pH = 2Toluene solution to obtain a hydrolyzate.(3) adjusting the pH of the hydrolyzate to neutral, extracting the organic layer three times with ethyl acetate,Washed three times, dried over anhydrous magnesium sulfate overnight and removed by rotary evaporation of ethyl acetate, To obtain 1,3-bis (hydroxybutyl) -1,1,3,3-tetramethyldisiloxane,The yield is about 83.7%.

References:

Shandong University;Zhang Jie;Li Jing CN106905356, 2017, A Location in patent:Paragraph 0064; 0065; 0066; 0067; 0069; 0070

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5931-17-9
119 suppliers
$60.00/100mg

References