![](/CAS/GIF/1477-55-0.gif)
1,3-Bis(aminomethyl)benzene synthesis
- Product Name:1,3-Bis(aminomethyl)benzene
- CAS Number:1477-55-0
- Molecular formula:C8H12N2
- Molecular Weight:136.19
![3-Cyanobenzaldehyde](/CAS/20180906/GIF/24964-64-5.gif)
24964-64-5
322 suppliers
$9.00/1g
![1,3-Bis(aminomethyl)benzene](/CAS/GIF/1477-55-0.gif)
1477-55-0
341 suppliers
$10.00/5g
Yield:1477-55-0 100%
Reaction Conditions:
with ammonia;hydrogen in methanol at 100; under 37503.8 Torr; for 5 h;
Steps:
1.5
1.5 Conversion of 3-formylbenzonitrile to 1,3-phenylenedimethanamine Simultaneous hydrogenation and reductive amination was carried out in batchreactor, containing 113 g of NH3 in MeOH (7 mol/l; d0.779), 0.7 g of Raney Coand 7 g of 3-formylbenzonitrile, ratio of NH3/aromatic is 19, at 100°C and 50 barof hydrogen during 5h. Yield was quantitative in metaxylenediamine.
References:
WO2017/97220,2017,A1 Location in patent:Page/Page column 24
![1,3-Dicyanobenzene](/CAS/GIF/626-17-5.gif)
626-17-5
305 suppliers
$10.00/1g
![3-CYANOBENZYLAMINE](/CAS/GIF/10406-24-3.gif)
10406-24-3
102 suppliers
$24.00/250mg
![1,3-Bis(aminomethyl)benzene](/CAS/GIF/1477-55-0.gif)
1477-55-0
341 suppliers
$10.00/5g
![1,3-Dicyanobenzene](/CAS/GIF/626-17-5.gif)
626-17-5
305 suppliers
$10.00/1g
![1,3-Bis(aminomethyl)benzene](/CAS/GIF/1477-55-0.gif)
1477-55-0
341 suppliers
$10.00/5g
![1,3-Dicyanobenzene](/CAS/GIF/626-17-5.gif)
626-17-5
305 suppliers
$10.00/1g
![1,3-Bis(aminomethyl)benzene](/CAS/GIF/1477-55-0.gif)
1477-55-0
341 suppliers
$10.00/5g
![3-CYANOBENZYLAMINE](/CAS/GIF/10406-24-3.gif)
10406-24-3
102 suppliers
$24.00/250mg