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17257-80-6

1-(3-Butyloxiranyl)ethanone synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 95 percent / 85percent m-chloroperbenzoic acid / CH2Cl2 / 0 deg C, then Rt, 2 h
2: 71 percent / 1.) oxalyl chloride, DMSO; 2.) Et3 N / CH2Cl2 / -60 deg C, 2 min, then -60 deg C, 15 min

References:

Corey, L. D.;Singh, S. M.;Oehlschlager, A. C. [Canadian Journal of Chemistry,1987,vol. 65,p. 1821 - 1827]