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ChemicalBook CAS DataBase List 1,3-Dichloro-2-ethylbenzene

1,3-Dichloro-2-ethylbenzene synthesis

7synthesis methods
-

Yield:33407-02-2 90%

Reaction Conditions:

Stage #1: 1,3-Dichlorobenzenewith sec.-butyllithium in tetrahydrofuran;cyclohexane at -75; for 0.75 h;
Stage #2: diethyl sulfate in tetrahydrofuran;cyclohexane;Cooling;

References:

Schlosser, Manfred;Heiss, Christophe;Marzi, Elena;Scopelliti, Rosario [European Journal of Organic Chemistry,2006,# 19,p. 4398 - 4404]