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54945-11-8

1,3-DIMETHYL-5-PYRAZOLIDONE synthesis

2synthesis methods
1-Pyrazolidinecarboxylic acid, 2,5-dimethyl-3-oxo-, 1,1-dimethylethyl ester

204197-22-8
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Yield:54945-11-8 55%

Reaction Conditions:

with trifluoroacetic acid in dichloromethane at 20;

References:

Gould, Eoin;Lebl, Tomas;Slawin, Alexandra M.Z.;Reid, Mark;Smith, Andrew D. [Tetrahedron,2010,vol. 66,# 46,p. 8992 - 9008] Location in patent:experimental part