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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

1,3-Dioxane, 5-(2-chloroethyl)-2,2-dimethyl- synthesis

3synthesis methods
2-allylpropane-1,3-diol

42201-43-4
8 suppliers
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1,3-Dioxane, 5-(2-chloroethyl)-2,2-dimethyl-

113998-32-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 89 percent / p-toluenesulfonic acid / benzene / 11 h / Heating
2: ozone / diethyl ether / 2 h / -78 °C
3: LiAlH4 / diethyl ether / 2 h / Ambient temperature
4: 89 percent / triphenylphosphine / CCl4 / 22 h / Heating

References:

Vite;Spencer [Journal of Organic Chemistry,1988,vol. 53,# 11,p. 2555 - 2560]

2-(2,2-Dimethyl-1,3-dioxan-5-yl)ethanol

102147-75-1
3 suppliers
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1,3-Dioxane, 5-(2-chloroethyl)-2,2-dimethyl-

113998-32-6
0 suppliers
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References
1,3-Dioxane, 2,2-dimethyl-5-(2-propen-1-yl)-

113999-09-0
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1,3-Dioxane, 5-(2-chloroethyl)-2,2-dimethyl-

113998-32-6
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References