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ChemicalBook CAS DataBase List 1,3-dioxepan-2-one

1,3-dioxepan-2-one synthesis

5synthesis methods
-

Yield:4427-94-5 97%

Reaction Conditions:

in acetonitrile

Steps:

11 EXAMPLE 11
EXAMPLE 11 0.01 mole of butylene chlorohydrin was added to a suspension of 0.012 moles of tetramethylammonium bicarbonate in 25 cm3 of acetonitrile, whereupon the procedure was as in Example 6. 1.13 g of butylene carbonate were thus obtained. The yield was about 97% (gas-liquid chromatographic analysis).

References:

Montedison S.p.A. US4226778, 1980, A

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