![](/CAS/GIF/102-04-5.gif)
1,3-Diphenylacetone synthesis
- Product Name:1,3-Diphenylacetone
- CAS Number:102-04-5
- Molecular formula:C15H14O
- Molecular Weight:210.27
![Benzyl bromide](/CAS/GIF/100-39-0.gif)
100-39-0
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![Phenylacetyl chloride](/CAS/GIF/103-80-0.gif)
103-80-0
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![1,3-Diphenylacetone](/CAS/GIF/102-04-5.gif)
102-04-5
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Yield:102-04-5 41 mmol
Reaction Conditions:
with bis(1,5-cyclooctadiene)nickel(0);magnesium chloride;zinc in acetonitrile at 20; for 12 h;Inert atmosphere;
Steps:
1.1 Step1
To just from the blast oven out of the three bottles of brominated Bian 100mmol,Anhydrous magnesium chloride 1.5 equivalents,Ligand bipyridine 0.15 equivalents,Activated Zinc Powder 3 Equivalent.Under nitrogen protection,Adding Ni (COD) 2 0.1 equivalent,After the next nitrogen protection,Add solvent acetonitrile,withAcid chloride.Reaction at room temperature for 12 h.After completion of the reaction,By column chromatography,Get the product41 mmol (1-1)
References:
Changchun Hai Purunsi Technology Co., Ltd.;Sun Keyi;Cai Hui CN107235858, 2017, A Location in patent:Paragraph 0032; 0034
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1788-31-4
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![1,3-Diphenylacetone](/CAS/GIF/102-04-5.gif)
102-04-5
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![1,3-Dithiolane,2,2-bis(phenylmethyl)-](/CAS/20180601/GIF/76312-47-5.gif)
76312-47-5
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![1,3-Diphenylacetone](/CAS/GIF/102-04-5.gif)
102-04-5
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![1,3-Dithiane, 2,2-bis(phenylmethyl)-](/CAS/20200611/GIF/40939-52-4.gif)
40939-52-4
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![1,3-Diphenylacetone](/CAS/GIF/102-04-5.gif)
102-04-5
290 suppliers
$9.00/10g