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1,4,6,9-tetraoxa-5$l^{4}-telluraspiro[4.4]nonane synthesis

1synthesis methods
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Yield:176-57-8 86%

Reaction Conditions:

with tellurium oxide;toluene-4-sulfonic acid1.) 120 deg C, 3 h ; 2.) 160 deg C;

References:

Badesha, Santokh S.;Monczka, Paul;Smith, Steven D. [Canadian Journal of Chemistry,1983,vol. 61,p. 2199 - 2202]