1,4-Bis(methylthio)naphthalene synthesis
- Product Name:1,4-Bis(methylthio)naphthalene
- CAS Number:10075-73-7
- Molecular formula:C12H12S2
- Molecular Weight:220.35
83-53-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique
1.2: 1 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique
2.2: 1 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
References:
Moon, Sanghun;Nishii, Yuji;Miura, Masahiro [Organic Letters,2019,vol. 21,# 1,p. 233 - 236]
624-92-0
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134-32-7
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10075-72-6
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1000210-73-0
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