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1,4-bis(tetrahydro-2-furyloxy)butane synthesis

2synthesis methods
-

Yield:76702-30-2 17%

Steps:

5 Example 5

Example 5 10 g of a mixture of 2-(4-hydroxybutoxy)tetrahydrofuran of the formula IIc (83%) and 1,4-bis(2-tetrahydrofuranyloxy)butane (17%) obtained as described in section (b) of Example 1 were hydrogenated at 100° C. and 150 bar in the presence of 1 g of a palladium catalyst (10% of Pd on activated carbon) for 10 hours.

References:

US5008408,1991,A