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ChemicalBook CAS DataBase List 1-(4-BROMO-2-FLUOROPHENYL)HYDRAZINE HYDROCHLORIDE

1-(4-BROMO-2-FLUOROPHENYL)HYDRAZINE HYDROCHLORIDE synthesis

1synthesis methods
-

Yield:299440-17-8 76.2%

Reaction Conditions:

Stage #1: 4-bromo-2-fluoroanilinewith hydrogenchloride;sodium nitrite in water at 0 - 5; for 0.166667 h;
Stage #2: with hydrogenchloride;tin(ll) chloride in water;cooling;

References:

Makhija, Mahindra T.;Kasliwal, Rajesh T.;Kulkarni, Vithal M.;Neamati, Nouri [Bioorganic and Medicinal Chemistry,2004,vol. 12,# 9,p. 2317 - 2333]

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