1-(4-bromophenoxy)-4-methanesulfonylbenzene synthesis
- Product Name:1-(4-bromophenoxy)-4-methanesulfonylbenzene
- CAS Number:83642-28-8
- Molecular formula:C13H11BrO3S
- Molecular Weight:327.19
Yield:83642-28-8 61%
Reaction Conditions:
Stage #1: 4-bromophenyl phenyl etherwith trifluorormethanesulfonic acid;C12H14INO5S in acetonitrile at 20;Inert atmosphere;Schlenk technique;Sealed tube;
Stage #2: methanesulfinic acid sodium saltwith sodium hydroxide in acetonitrile at 120; for 4 h;Inert atmosphere;Schlenk technique;Sealed tube;
References:
Chen, Yixuan;Gu, Yuefei;Meng, Huan;Shao, Qianzhen;Xu, Zhenchuang;Bao, Wenjing;Gu, Yucheng;Xue, Xiao-Song;Zhao, Yanchuan [Angewandte Chemie - International Edition,2022,vol. 61,# 28,art. no. E202201240][Angew. Chem.,2022,vol. 134,# 28] Location in patent:supporting information
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