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1-(4-bromophenyl)propane-1,2-dione synthesis

10synthesis methods
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Yield:10557-20-7 90%

Reaction Conditions:

Stage #1: p-bromopropiophenonewith [hydroxy(p-nitrobenzenesulfonyloxy)iodo]benzene for 0.025 h;microwave irradiation;
Stage #2: with pyridine N-oxide for 0.00833333 h;microwave irradiation;

References:

Lee, Jong Chan;Park, Hong-Jun;Park, Jin Young [Tetrahedron Letters,2002,vol. 43,# 32,p. 5661 - 5664]