1,4-Cyclohexadiene-1-methanol, 4-methyl- synthesis
1synthesis methods
- Product Name:1,4-Cyclohexadiene-1-methanol, 4-methyl-
- CAS Number:67086-95-7
- Molecular formula:C8H12O
- Molecular Weight:124.18
Yield:67086-95-7 73%
Reaction Conditions:
with 1,2-bis(diphenylphosphanyl)ethane;cobalt(II) dibromide;zinc(II) iodide;zinc in tetrahydrofuran at 50;Inert atmosphere;
References:
Touge, Taichiro;Hakamata, Tomohiko;Nara, Hideki;Kobayashi, Tohru;Sayo, Noboru;Saito, Takao;Kayaki, Yoshihito;Ikariya, Takao [Journal of the American Chemical Society,2011,vol. 133,# 38,p. 14960 - 14963] Location in patent:supporting information; experimental part