1,4-DIIODOTETRAFLUOROBENZENE synthesis
- Product Name:1,4-DIIODOTETRAFLUOROBENZENE
- CAS Number:392-57-4
- Molecular formula:C6F4I2
- Molecular Weight:401.87
327-54-8
236 suppliers
$10.00/10g
392-57-4
96 suppliers
$24.00/1g
Yield:392-57-4 68%
Reaction Conditions:
with iodine
Steps:
5 1,2,4,5-Tetrafluoro-3,6-diiodobenzene
EXAMPLE 5 1,2,4,5-Tetrafluoro-3,6-diiodobenzene 1,2,4,5-Tetrafluorobenzene(11.3 g, 75 mmol) and iodine(21.9 g, 86 mmol) gave 3,6-diiodo-1,2,4,5-tetrafluorobenzene (20.5 g, 68%); m.p. 109°-111° C. (lit;2 109°-111° C.); (Found: C. 17.59; H, 0; N, 0. C6 F4 I2 requires C, 17.93; H, 0; N, 0%); δF -118.0 (4F, s,1-F, 2-F, 3-F, 4-F); δC 72.9 (2C, t, 2 JC-F 27.9, 3C, 6-C) and 146.6 (4C, m, 1 JC-F 250.4, 1-C, 2C, 4-C, 5-C); m/z (EI+) 402 (M+, 46.7%).
References:
BNFL Fluorochemicals Ltd US5734073, 1998, A
327-54-8
236 suppliers
$10.00/10g
392-57-4
96 suppliers
$24.00/1g
5243-24-3
17 suppliers
$95.00/250 mg
327-54-8
236 suppliers
$10.00/10g
7664-93-9
6 suppliers
$21.64/1003
7446-11-9
65 suppliers
$145.00/40g
7553-56-2
618 suppliers
$18.00/25g
392-57-4
96 suppliers
$24.00/1g