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ChemicalBook CAS DataBase List 1-(5-Bromomethyl-2-nitro-phenyl)-ethanone
99821-59-7

1-(5-Bromomethyl-2-nitro-phenyl)-ethanone synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: thionyl chloride / Inert atmosphere
2.1: magnesium / Inert atmosphere
2.2: Inert atmosphere
3.1: hydrogenchloride; water / Inert atmosphere
4.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

References:

Szychowski, Janek;Mahdavi, Alborz;Hodas, Jennifer J. L.;Bagert, John D.;Ngo, John T.;Landgraf, Peter;Dieterich, Daniela C.;Schuman, Erin M.;Tirrell, David A. [Journal of the American Chemical Society,2010,vol. 132,# 51,p. 18351 - 18360]