1,5-DECADIYNE synthesis
- Product Name:1,5-DECADIYNE
- CAS Number:53963-03-4
- Molecular formula:C10H14
- Molecular Weight:134.22
628-16-0
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$98.09/2g
53963-03-4
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$48.00/1mL
Yield:-
Reaction Conditions:
in carbon dioxide
Steps:
Preparation of (Z,Z)-7,11-hexadecadienyl Acetate 1,5-Decadiyne
The low boiling 1,5-hexadiyne is collected in dry-ice cooled receiver, 1,5-decadiyne, nD21 1.4550, is collected at 84°-86°/30 torr and amounts to approximately 400 grams (50% based on starting 1,5-hexadiyne). 5,9-tetradecadiyne is collected at 110°-112°/2 torr and amounts to approximately 180 grams. (15% based on starting 1,5-hexadiyne). The yields of 1,5-decadiyne range between 40 and 60%.
References:
Story Chemical Corporation US3996270, 1976, A
68274-97-5
41 suppliers
$56.10/1g
53963-03-4
53 suppliers
$48.00/1mL