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19162-00-6

1,5-dimethylhex-4-enyl acetate synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 82 percent / HBF4 / CH2Cl2; diethyl ether / 0.5 h / -30 °C
2: t-BuOK / dimethylsulfoxide / 24 h / 20 °C

References:

Badet,B.;Julia,M.;Mallet,J.M. [Tetrahedron,1988,vol. 44,p. 2913]