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1,6-anhydro-2-deoxy-2-iodo-D-glucopyranose synthesis

5synthesis methods
-

Yield:139437-39-1 65%

Reaction Conditions:

Stage #1: D-glucalwith 3 Angstroem MS;bis(tri-n-butyltin)oxide in acetonitrile; for 3 h;Heating;
Stage #2: with iodine in dichloromethane at 0; for 0.25 h;Further stages.;

References:

Hawley, Joanne;Bampos, Nick;Aboitiz, Nuria;Jimenez-Barbero, Jesus;Lopez De La Paz, Manuela;Sanders, Jeremy K. M.;Carmona, Pedro;Vicent, Cristina [European Journal of Organic Chemistry,2002,# 12,p. 1925 - 1936]