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1,6-Hexanediol, monoacetate synthesis

9synthesis methods
1-Hexanol, 6-([1,1'-biphenyl]-4-ylmethoxy)-, 1-acetate

1426306-47-9
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1,6-Hexanediol, monoacetate

68750-24-3
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Yield:68750-24-3 97%

Reaction Conditions:

with tert.-butylnitrite;oxygen;2,3-dicyano-5,6-dichloro-p-benzoquinone in chlorobenzene at 100; under 760.051 Torr; for 6.5 h;

References:

Shen, Zhenlu;Sheng, Lili;Zhang, Xiaochu;Mo, Weimin;Hu, Baoxiang;Sun, Nan;Hu, Xinquan [Tetrahedron Letters,2013,vol. 54,# 12,p. 1579 - 1583]