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172915-62-7

1,8-bis(MethoxyMethoxy)naphthalene synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: potassium hydroxide / 1 h / 260 °C
1.2: 0.5 h / 100 °C
2.1: sodium hydride / diethyl ether; N,N-dimethyl-formamide / 0 °C
2.2: 6 h / 0 - 20 °C

References:

US2013/41169,2013,A1