![](/CAS/GIF/56403-09-9.gif)
1,8-diazacyclotetradecane-2,9-dione synthesis
- Product Name:1,8-diazacyclotetradecane-2,9-dione
- CAS Number:56403-09-9
- Molecular formula:C12H22N2O2
- Molecular Weight:226.32
![6-Aminocaproic acid](/CAS/GIF/60-32-2.gif)
60-32-2
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 83 percent / 4 M NaOH / 4 h / 0 - 20 °C
2: DCC / dioxane / 24 h / 0 °C
3: aq. NaHCO3 / 1,2-dimethoxy-ethane / 5 h / 20 °C
4: 90 percent / DCC / dimethylformamide / 3 h / 0 - 20 °C
5: 33percent HBr / acetic acid / 2 h / 20 °C
6: pyridine / dimethylformamide / 4 h / 60 °C
References:
Mikhura, I. V.;Formanovskii, A. A. [Chemistry of Heterocyclic Compounds,1992,vol. 28,# 2,p. 205 - 212][Khimiya Geterotsiklicheskikh Soedinenii,1992,# 2,p. 247 - 255]
![6-(BOC-AMINO)CAPROIC ACID N-SUCCINIMIDYL ESTER](/CAS/GIF/51513-80-5.gif)
51513-80-5
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![Boc-6-AMinocaproic acid](/CAS/GIF/6404-29-1.gif)
6404-29-1
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![1,8-diazacyclotetradecane-2,9-dione](/CAS/GIF/56403-09-9.gif)
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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![1,8-diazacyclotetradecane-2,9-dione](/CAS/GIF/56403-09-9.gif)
56403-09-9
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