![](/CAS/GIF/6306-07-6.gif)
1-ACENAPHTHENOL synthesis
- Product Name:1-ACENAPHTHENOL
- CAS Number:6306-07-6
- Molecular formula:C12H10O
- Molecular Weight:170.21
![1-Acenaphthenone](/CAS/GIF/2235-15-6.gif)
2235-15-6
120 suppliers
$100.00/1 g
![1-ACENAPHTHENOL](/CAS/GIF/6306-07-6.gif)
6306-07-6
89 suppliers
$26.50/1g
Yield: 94.2%
Reaction Conditions:
with hydrogen in methanol at 100; under 30003 Torr;Autoclave;Temperature;
Steps:
2.1
1) In a 1000 ml autoclave, 700 ml of methanol was added as a solvent,Followed by the addition of 168 gl-acenaphthene, 13 g hydrogenation catalyst nickel catalyst AMG-1200; added to complete, sealed reactor,First use the nitrogen to replace the kettle air twice, through the H2 to the pressure4.OMPa, open the stirring, heating to 100 ° C to react, the reaction to no hydrogen,1-naphthenaphthene was removed and the reaction was stopped,Followed by column purification of 1 - hydroxy acenaphthalene pure product 160.14g, the yield was 94.2%
References:
Wang Jiju CN106397116, 2017, A Location in patent:Paragraph 0012
![Acenaphthene](/CAS/GIF/83-32-9.gif)
83-32-9
259 suppliers
$14.00/5g
![1-ACENAPHTHENOL](/CAS/GIF/6306-07-6.gif)
6306-07-6
89 suppliers
$26.50/1g
![1-Acenaphthenone](/CAS/GIF/2235-15-6.gif)
2235-15-6
120 suppliers
$100.00/1 g
![ACENAPHTHYLENE](/CAS/GIF/208-96-8.gif)
208-96-8
244 suppliers
$5.00/250mg
![1-ACENAPHTHENOL](/CAS/GIF/6306-07-6.gif)
6306-07-6
89 suppliers
$26.50/1g
![Acenaphthene](/CAS/GIF/83-32-9.gif)
83-32-9
259 suppliers
$14.00/5g
![1-ACENAPHTHENOL](/CAS/GIF/6306-07-6.gif)
6306-07-6
89 suppliers
$26.50/1g
![Acenaphthenequinone](/CAS/GIF/82-86-0.gif)
82-86-0
207 suppliers
$10.00/1g
![DECACYCLENE](/CAS/GIF/191-48-0.gif)
191-48-0
67 suppliers
$500.13/5MG
![1-ACENAPHTHENOL](/CAS/GIF/6306-07-6.gif)
6306-07-6
89 suppliers
$26.50/1g
![Acenaphthene](/CAS/GIF/83-32-9.gif)
83-32-9
259 suppliers
$14.00/5g
![ACENAPHTHYLENE](/CAS/GIF/208-96-8.gif)
208-96-8
244 suppliers
$5.00/250mg