ChemicalBook CAS DataBase List 1-Allylcyclopropanecarboxylic acid

1-Allylcyclopropanecarboxylic acid synthesis

4synthesis methods

Product Name:1-Allylcyclopropanecarboxylic acid
CAS Number:80360-57-2
Molecular formula:C7H10O2
Molecular Weight:126.15

tert-Butyl 1-allylcyclopropanecarboxylate

108546-98-1
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Yield: 90%

Reaction Conditions:

with trifluoroacetic acid

Steps:

3 1-Allylcyclopropanecarboxylic acid STR16
1-Allylcyclopropanecarboxylic acid STR16 24.0 g (0.13 mol) of tert-butyl 1-allylcyclopropanecarboxylate (prepared according to Example 1a) were reacted with 14.9 g (0.13 mol) of trifluoroacetic acid similarly to Example 1c. Yield: 90%; colorless oil.

References:

BASF Aktiengesellschaft US5371268, 1994, A

106-95-6 Synthesis