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ChemicalBook CAS DataBase List 1-Aminonaphthalene-2-carboxaldehyde
176853-41-1

1-Aminonaphthalene-2-carboxaldehyde synthesis

4synthesis methods
2-(DIMETHYLAMINO)VINYL-1-NITRONAPHTHAL&

176853-40-0
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1-Aminonaphthalene-2-carboxaldehyde

176853-41-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 85 percent / sodium periodate / tetrahydrofuran; H2O / 2 h / 25 °C
2: 77 percent / Fe powder, conc. HCl / ethanol; acetic acid; H2O / 1) reflux, 15 min; 2) 25 deg C, 25 min

References:

Riesgo, Elvira C.;Jin, Xiaoqing;Thummel, Randolph P. [Journal of Organic Chemistry,1996,vol. 61,# 9,p. 3017 - 3022]