1-Boc-2-(hydroxydimethylsilyl)pyrrole, 97% synthesis
- Product Name:1-Boc-2-(hydroxydimethylsilyl)pyrrole, 97%
- CAS Number:879904-82-2
- Molecular formula:C11H19NO3Si
- Molecular Weight:241.36
5176-27-2
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$10.00/1g
75-78-5
369 suppliers
$15.00/5G
879904-82-2
21 suppliers
$64.59/250mg
Yield:879904-82-2 50%
Reaction Conditions:
Stage #1: N-tert-butyloxycarbonyl-pyrrolewith lithium diisopropyl amide in tetrahydrofuran;hexane at -71; for 6 h;
Stage #2: dimethylsilicon dichloride in tetrahydrofuran;hexane at -71 - 20; for 10 h;
Stage #3: with sodium hydrogencarbonate in tetrahydrofuran;hexane;water;cooling;Further stages.;
References:
Denmark, Scott E.;Baird, John D.;Regens, Christopher S. [Journal of Organic Chemistry,2008,vol. 73,# 4,p. 1440 - 1455]
5176-27-2
180 suppliers
$10.00/1g
879904-82-2
21 suppliers
$64.59/250mg