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ChemicalBook CAS DataBase List 1-bromo-2,3,5-trimethylBenzene
31053-99-3

1-bromo-2,3,5-trimethylBenzene synthesis

6synthesis methods
209684-76-4 Synthesis
2,3,5-Trimethylphenyl Trifluoromethanesulfonate

209684-76-4
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Yield:31053-99-3 80%

Reaction Conditions:

with potassium fluoride;tris-(dibenzylideneacetone)dipalladium(0);t-BuBrettPhos;potassium bromide in 1,4-dioxane at 130; for 16 h;Inert atmosphere;

References:

Pan, Jun;Wang, Xinyan;Zhang, Yong;Buchwald, Stephen L. [Organic Letters,2011,vol. 13,# 18,p. 4974 - 4976] Location in patent:supporting information; experimental part