1-BROMO-4-(1H,1H,2H,2H-PERFLUOROPENTYL)BENZENE synthesis
- Product Name:1-BROMO-4-(1H,1H,2H,2H-PERFLUOROPENTYL)BENZENE
- CAS Number:195324-88-0
- Molecular formula:C16H8BrF17
- Molecular Weight:603.11
Yield:195324-88-0 46%
Reaction Conditions:
Stage #1: 2-(n-perfluorooctyl)ethyl iodidewith chloro-trimethyl-silane;ethylene dibromide;zinc in tetrahydrofuran at 20; for 15 h;
Stage #2: 1,4-bromoiodobenzene in tetrahydrofuran at 45; for 12 h;
References:
Curran, Dennis P.;Oderaotoshi, Yoji [Tetrahedron,2001,vol. 57,# 24,p. 5243 - 5253]
673-40-5
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195324-88-0
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