1-bromo-dibenzofuran-4-ol synthesis

3synthesis methods

Product Name:1-bromo-dibenzofuran-4-ol
CAS Number:873974-43-7
Molecular formula:C12H7BrO2
Molecular Weight:263.09

100124-06-9 Synthesis

100124-06-9
398 suppliers
$6.00/1g

873974-43-7
19 suppliers
$176.00/250 mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: urea hydrogen peroxide adduct / acetonitrile / 20 °C / Cooling with ice; Inert atmosphere
2: 1H-imidazole / dichloromethane / 18 h / 20 °C / Inert atmosphere
3: N-Bromosuccinimide / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere
4: cesium fluoride / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

References:

Wern, Caroline;Ehrenreich, Christian;Joosten, Dominik;Stein, Thorsten vom;Buchholz, Herwig;König, Burkhard [European Journal of Organic Chemistry,2018,vol. 2018,# 41,p. 5644 - 5656]

19261-06-4
38 suppliers
$168.00/250 mg

873974-43-7
19 suppliers
$176.00/250 mg

References

19261-06-4
38 suppliers
$168.00/250 mg

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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64-19-7 Synthesis

64-19-7
1540 suppliers
$10.00/25ML

873974-43-7
19 suppliers
$176.00/250 mg

References