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126840-36-6

1-BROMOOCTANE-D17 synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 89.2 percent / LiAlD4 / diethyl ether / 8 h / Heating
2: 84 percent / red phosphorous, Br2 / 85 - 90 °C

References:

Lipinski, K.;Lipinska, T.;Suszko-Purzycka, A.;Rykowski, A. [Polish Journal of Chemistry,1993,vol. 67,# 4,p. 667 - 672]

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