1-butyl-3-nitrobenzene synthesis

10synthesis methods

Product Name:1-butyl-3-nitrobenzene
CAS Number:20651-76-7
Molecular formula:C10H13NO2
Molecular Weight:179.22

585-79-5 Synthesis

585-79-5
7 suppliers
$15.00/1g

69190-62-1 Synthesis

2-BUTYL-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE

69190-62-1
90 suppliers
$21.00/5g

20651-76-7
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Yield:20651-76-7 91%

Reaction Conditions:

with tris-(dibenzylideneacetone)dipalladium⁽⁰⁾;sodium t-butanolate;ruphos in water;toluene at 80; for 24 h;Inert atmosphere;Suzuki coupling;

References:

Yang, Chu-Ting;Zhang, Zhen-Qi;Tajuddin, Hazmi;Wu, Chen-Cheng;Liang, Jun;Liu, Jing-Hui;Fu, Yao;Czyzewska, Maria;Steel, Patrick G.;Marder, Todd B.;Liu, Lei [Angewandte Chemie - International Edition,2012,vol. 51,# 2,p. 528 - 532] Location in patent:supporting information; experimental part