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ChemicalBook CAS DataBase List 1-Chloro-2,3,4,6-tetrafluorobenzene

1-Chloro-2,3,4,6-tetrafluorobenzene synthesis

8synthesis methods
-

Yield:1835-61-6 60% ,5172-06-5 8% ,769-37-9 12%

Reaction Conditions:

with tetrabutylammonium triphenyldifluorosilicate;HSiPh3 in tetrahydrofuran;benzene-d6 at 60; for 40 h;Inert atmosphere;Sealed tube;

References:

Kikushima, Kotaro;Grellier, Mary;Ohashi, Masato;Ogoshi, Sensuke [Angewandte Chemie - International Edition,2017,vol. 56,# 51,p. 16191 - 16196][Angew. Chem.,2017,vol. 129,p. 16409 - 16414,6] Location in patent:supporting information