![](/CAS/20150408/GIF/168967-40-6.gif)
1-cyclooctyl-iMidazole synthesis
- Product Name:1-cyclooctyl-iMidazole
- CAS Number:168967-40-6
- Molecular formula:C11H18N2
- Molecular Weight:178.27
![Formaldehyde](/CAS/GIF/50-00-0.gif)
50-00-0
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![Cyclooctylamine](/CAS/GIF/5452-37-9.gif)
5452-37-9
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![1-cyclooctyl-iMidazole](/CAS/20150408/GIF/168967-40-6.gif)
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Yield:168967-40-6 29%
Reaction Conditions:
Stage #1: formaldehyd;Glyoxal;cyclooctylaminewith phosphoric acid in 1,4-dioxane;water at 80; pH=2; for 0.5 h;
Stage #2: with ammonium chloride in 1,4-dioxane;water at 100; for 3 h;Further stages.;
References:
Perry, Marc C.;Cui, Xiuhua;Powell, Mark T.;Hou, Duen-Ren;Reibenspies, Joseph H.;Burgess, Kevin [Journal of the American Chemical Society,2003,vol. 125,# 1,p. 113 - 123]