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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List (1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE

(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE synthesis

3synthesis methods
For the synthesis of the parent and the 2-monoalkyl-substituted compounds, reduction of ethyl 3- chloropropionate with sodium–potassium alloy in the presence of chlorotrimethylsilane in ether. A recent modification using ultrasound irradiation is much more convenient and more widely applicable. Other substituted derivatives are prepared by cyclopropanation of alkyl silyl ketene acetals with the Furukawa reagent (diiodomethane/diethylzinc).
7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
373 suppliers
$19.00/5g

Magnesium, (1-ethoxycyclopropanolato)iodo-

74592-24-8
0 suppliers
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(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE

27374-25-0
205 suppliers
$13.00/250mg

1-ethoxycyclopropanol

13837-45-1
31 suppliers
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-

Yield:27374-25-0 75%

Reaction Conditions:

with zinc(II) iodide in diethyl ether for 48 h;Heating;

References:

Salauen, Jacques;Bennani, Fatima;Compain, Jean-Claude;Fadel, Antoine;Ollivier, Jean [Journal of Organic Chemistry,1980,vol. 45,# 21,p. 4129 - 4135]

FullText

Chlorotrimethylsilane

75-77-4
567 suppliers
$5.04/10

Ethyl 3-chloropropionate

623-71-2
145 suppliers
$27.57/250mgs:

(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE

27374-25-0
205 suppliers
$13.00/250mg

References
7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
373 suppliers
$19.00/5g

1-ethoxycyclopropanol

13837-45-1
31 suppliers
inquiry

(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE

27374-25-0
205 suppliers
$13.00/250mg

References

(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE Related Search:

Cyclopropane TRIMETHYLSILANE