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ChemicalBook CAS DataBase List 1-ETHYNYL-2,3-DIMETHYL-BENZENE
767-87-3

1-ETHYNYL-2,3-DIMETHYL-BENZENE synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: (bis(tricyclohexyl)phosphine)palladium(II) dichloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / 2-methyltetrahydrofuran / 30 °C / Inert atmosphere
2: caesium carbonate / ethanol / 30 °C / Inert atmosphere

References:

Shanghai Bozhi Yan Xin Pharmaceutical Co., Ltd.;Chen Jian;Qiao Yanhe;Ying Shuhuan CN108147999, 2018, A