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1-ETHYNYL-2,4-DIMETHYL-BENZENE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / N,N-dimethyl-formamide / 8 h / 90 °C / Inert atmosphere
2: potassium carbonate / methanol / 10 h / 20 °C

References:

DIC Co., Ltd.;HORIGUCHI, MASAHIRO;HAYASHI, MASANAO;KUSUMOTO, TETSUO JP2015/40174, 2015, A

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