1-Heptatriacotanol synthesis
- Product Name:1-Heptatriacotanol
- CAS Number:105794-58-9
- Molecular formula:C37H76O
- Molecular Weight:537
2424-92-2
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105794-58-9
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Yield:-
Steps:
Multi-step reaction with 10 steps
1: sulfuric acid
2: lithium aluminium tetrahydride / tetrahydrofuran
3: 1H-imidazole / N,N-dimethyl-formamide
4: 1H-imidazole; iodine; triphenylphosphine / toluene
5: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran
6: hydrogen; palladium on activated charcoal / ethyl acetate
7: pyridinium chlorochromate / dichloromethane
8: sodium hexamethyldisilazane / tetrahydrofuran
9: tetrabutyl ammonium fluoride / tetrahydrofuran
10: hydrogen; palladium 10% on activated carbon / ethyl acetate
References:
Zhang, Hong-Yan;Yamakawa, Yu-Ichiro;Matsuya, Yuji;Toyooka, Naoki;Tohda, Chihiro;Awale, Suresh;Li, Feng;Kadota, Shigetoshi;Tezuka, Yasuhiro [Bioorganic and Medicinal Chemistry Letters,2014,vol. 24,# 2,p. 604 - 608]
42235-38-1
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105794-58-9
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7735-43-5
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105794-58-9
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