ChemicalBook CAS DataBase List 1-HYDROXY-CYCLOHEXANECARBOXAMIDINE

1-HYDROXY-CYCLOHEXANECARBOXAMIDINE synthesis

3synthesis methods

Product Name:1-HYDROXY-CYCLOHEXANECARBOXAMIDINE
CAS Number:781569-43-5
Molecular formula:C7H14N2O
Molecular Weight:142.2

Cyclohexanecarboximidic acid, 1-hydroxy-, methyl ester, hydrochloride (1:1)

7500-68-7
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781569-43-5
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Yield:-

Reaction Conditions:

with ammonia in methanol at -30 - 20;

Steps:

5.3 step 3

The hydrochloride (8 g) of compound 5-3 was suspended in methanol (100 mL),Ammonia gas was introduced at -30°C for 30 minutes, and the temperature of the reaction solution was slowly raised to 20°C and stirred for 12 hours.The reaction solution was concentrated under reduced pressure to obtain crude compound 5-4, which was directly used in the next step.

References:

WO2023/1282,2023,A1 Location in patent:Page/Page column 27-29

Cyclohexanecarbonitrile, 1-[(trimethylsilyl)oxy]-

24731-36-0
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781569-43-5
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References

108-94-1 Synthesis

108-94-1
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$12.00/50g

781569-43-5
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References

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