1-(hydroxymethyl)Cyclobutanecarboxylic acid synthesis
- Product Name:1-(hydroxymethyl)Cyclobutanecarboxylic acid
- CAS Number:114671-90-8
- Molecular formula:C6H10O3
- Molecular Weight:130.14
3779-29-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: lithium tri-(tert-butoxy)aluminum hydride / tetrahydrofuran / 12 h / -78 - 20 °C
2: sodium hydroxide / 1,4-dioxane; water / 3 h / 0 - 20 °C
References:
Xiao, Kai-Jiong;Lin, David W.;Miura, Motofumi;Zhu, Ru-Yi;Gong, Wei;Wasa, Masayuki;Yu, Jin-Quan [Journal of the American Chemical Society,2014,vol. 136,# 22,p. 8138 - 8142]
1195-81-9
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