1-iodo-3-Methoxy-2-Methylbenzene synthesis
- Product Name:1-iodo-3-Methoxy-2-Methylbenzene
- CAS Number:21093-09-4
- Molecular formula:C8H9IO
- Molecular Weight:248.06
19500-02-8
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Yield:21093-09-4 70%
Reaction Conditions:
Stage #1: 2-methyl-3-methoxyanilinewith hydrogenchloride;sodium nitrite in tetrahydrofuran;water at 0; for 0.333333 h;Inert atmosphere;
Stage #2: with potassium iodide in tetrahydrofuran;water at 0; for 24 h;Inert atmosphere;
References:
Khatri, Hem Raj;Zhu, Jianglong [Chemistry - A European Journal,2012,vol. 18,# 39,p. 12232 - 12236] Location in patent:supporting information