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1-Iodo-3-(trimethoxymethyl)benzene synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 90 percent / AlCl3 / 48 h / 60 °C
2: 85 percent / collidine, AgNO3 / acetonitrile / 4 h / Ambient temperature

References:

Breslow, Ronald;Pandey, P. S. [Journal of Organic Chemistry,1980,vol. 45,# 4,p. 740 - 741]