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ChemicalBook CAS DataBase List 1-Iodo-4-(1-propen-2-yl)benzene

1-Iodo-4-(1-propen-2-yl)benzene synthesis

5synthesis methods
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Yield:561023-21-0 81%

Reaction Conditions:

Stage #1: Methyltriphenylphosphonium bromidewith n-butyllithium in tetrahydrofuran;hexane at 0;Inert atmosphere;
Stage #2: 4-Iodoacetophenone in tetrahydrofuran;hexane at 0 - 20;Inert atmosphere;

References:

Chen, Lu;He, Runfa;Huang, Yubing;Li, Jiaming;Li, Jian;Li, Yibiao;Liu, Jiasheng;Liu, Yang [Organic Letters,2022,vol. 24,# 8,p. 1620 - 1625] Location in patent:supporting information