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ChemicalBook CAS DataBase List 1-METHANESULFONYL-PIPERIDINE-3-CARBOXYLIC ACID

1-METHANESULFONYL-PIPERIDINE-3-CARBOXYLIC ACID synthesis

1synthesis methods
349625-89-4 Synthesis
1-METHANESULFONYL-PIPERIDINE-3-CARBOXYLIC ACID ETHYL ESTER

349625-89-4
18 suppliers
$497.24/5MG

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Yield:702670-29-9 39%

Reaction Conditions:

Stage #1: ethyl 1-(methylsulfonyl)piperidine-3-carboxylatewith water;sodium hydroxide in methanol at 0 - 20; for 6 h;
Stage #2: with hydrogenchloride in water; pH=3;

References:

WO2007/29587,2007,A1 Location in patent:Page/Page column 67

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