ChemicalBook CAS DataBase List 1-METHOXY-2-BUTANOL

1-METHOXY-2-BUTANOL synthesis

9synthesis methods

Product Name:1-METHOXY-2-BUTANOL
CAS Number:53778-73-7
Molecular formula:C5H12O2
Molecular Weight:104.15

106-88-7 Synthesis

106-88-7
155 suppliers
$15.00/25mL

67-56-1 Synthesis

67-56-1
738 suppliers
$7.29/5ml-f

15467-25-1
46 suppliers
$45.00/50mg

53778-73-7
45 suppliers
$15.00/1g

Yield: 38% ， 58%

Reaction Conditions:

with graphite oxide at 20; for 1 h;

Steps:

General procedure for the alcoholysis of epoxides:
General procedure: To a solution of epoxide(1 mmol) and alcohol (5 mmol) was added 1 mg of graphite oxide (GO) at room temperature and the mixture stirred for the time indicated in Table 2 prior to GC/MS analysis. CH₂Cl₂ was added and the mixture was filtered and evaporated under reduced pressure. Pure products were isolated by flash column chromatography using hexane/EtOAc (6:1) as eluent.

References:

Mirza-Aghayan, Maryam;Alizadeh, Mahdi;Molaee Tavana, Mahdieh;Boukherroub, Rabah [Tetrahedron Letters,2014,vol. 55,# 49,p. 6694 - 6697]