ChemicalBook CAS DataBase List 1-METHYLCYCLOHEXANECARBONITRILE

1-METHYLCYCLOHEXANECARBONITRILE synthesis

6synthesis methods

Product Name:1-METHYLCYCLOHEXANECARBONITRILE
CAS Number:62718-34-7
Molecular formula:C8H13N
Molecular Weight:123.2

14064-13-2
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62718-34-7
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Yield:62718-34-7 99%

Reaction Conditions:

Stage #1: (1-methylcyclohexyl)methanolwith 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical;1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione in dichloromethane at 20; for 1 h;Inert atmosphere;
Stage #2: with ammonia;iodine in dichloromethane;water at 20; for 3 h;Inert atmosphere;

References:

Shimojo, Hiroyuki;Moriyama, Katsuhiko;Togo, Hideo [Synthesis,2013,vol. 45,# 15,art. no. SS-2013-F0311-OP,p. 2155 - 2164]

590-67-0 Synthesis