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ChemicalBook CAS DataBase List (1-methylpyrrolidin-3-yl)methanol
5021-33-0

(1-methylpyrrolidin-3-yl)methanol synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: sodium ethylate; xylene
2: Raney nickel / 100 °C / 110326 Torr / Hydrogenation
3: lithium alanate; diethyl ether
4: water; sulfuric acid; sodium periodate / Hydrieren der nach Entfernen der Schwefelsaeure erhaltenen Reaktionsloesung an Raney-Nickel bei 120grad/125 at

References:

MASCH;PETERSEN [Arzneimittel-Forschung/Drug Research,1959,vol. 9,p. 715 - 717]

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