![](/CAS/GIF/38746-10-0.gif)
1-METHYLQUINOLIUM METHYL SULFATE synthesis
- Product Name:1-METHYLQUINOLIUM METHYL SULFATE
- CAS Number:38746-10-0
- Molecular formula:C11H13NO4S
- Molecular Weight:255.29
![Quinoline](/CAS/GIF/91-22-5.gif)
91-22-5
384 suppliers
$10.00/25g
![Dimethyl sulfate](/CAS/GIF/77-78-1.gif)
77-78-1
290 suppliers
$22.00/25g
![1-METHYLQUINOLIUM METHYL SULFATE](/CAS/GIF/38746-10-0.gif)
38746-10-0
15 suppliers
$39.89/250mg
Yield:38746-10-0 100%
Reaction Conditions:
in acetonitrile at 40; for 24 h;
Steps:
Method A
General procedure: In a 30mL round bottomed flask, a mixtureof 8-methylquinoline (1.4 g, 10mmol) and dimethyl sulfate(2.5 g, 20mmol) was heated at 60 °C for 15 h. The precipitatedsolid was washed with THF (20 mL) to afford 1,8-dimethylquinoliniummethylsulfate 2a' (1.78 g, 6.6mmol, 66%) as a white solid. When other reaction conditions or substrates were used, reactions were conducted in a similar way.
References:
Iwai, Kento;Yokoyama, Soichi;Asahara, Haruyasu;Nishiwaki, Nagatoshi [Bulletin of the Chemical Society of Japan,2020,vol. 93,# 1,p. 50 - 57]