ChemicalBook CAS DataBase List 1-(Naphthalen-2-yl)ethanaMine HCl

1-(Naphthalen-2-yl)ethanaMine HCl synthesis

6synthesis methods

Product Name:1-(Naphthalen-2-yl)ethanaMine HCl
CAS Number:39110-76-4
Molecular formula:C12H14ClN
Molecular Weight:207.6993

939-27-5 Synthesis

939-27-5
88 suppliers
$16.00/1g

39110-76-4
19 suppliers
$110.00/1g

Yield:39110-76-4 50%

Reaction Conditions:

Stage #1: 2-ethylnaphthalenewith Benzophenone imine;copper(l) iodide;1,10-Phenanthroline;di-tert-butyl peroxide in chlorobenzene at 90; for 48 h;Inert atmosphere;Sealed tube;
Stage #2: with hydrogenchloride in methanol;water;chlorobenzene at 40; for 15 h;Inert atmosphere;Sealed tube;

References:

Kramer, S?ren [Organic Letters,2019,vol. 21,# 1,p. 65 - 69] Location in patent:supporting information

93-08-3 Synthesis